Question 5 of 7: Copper Wire Drawing — Penultimate Die Diameter for a Strength + Ductility Spec; Dislocations in Cold Rolling
Nivaar worked solution (AI-drafted; not reviewed by a licensed engineer)
Notes on this paper
National Exam 04-BS-11, Properties of Materials — May 2019 sitting (the cover page and every page footer read “04-BS-11, May2019”). 3 hours, closed-book examination (Casio/Sharp calculator only). Notes on the paper state that candidates are to
attempt five, and only five, questions, with only the first five appearing in the answer book marked and
all questions of equal value. All seven questions are solved below for completeness.
Reference texts: Callister & Rethwisch, Materials Science and Engineering:
An Introduction, 9th ed. (crystal structure and Miller indices; tensile testing and true strain;
hardness testing; solid solutions and grain size; phase diagrams and the lever rule; dislocations and
cold work; polymer molecular weight and viscoelastic behaviour; TTT diagrams and heat treatment;
fracture/fatigue).
Page-1 data used below: atomic masses (g/mol) H 1.01, C 12.01,
Mo 95.94; $N_A=0.602\times10^{24}$ mol$^{-1}$; cold work $CW=(A_0-A_f)/A_0$; grain size
$N=2^{n-1}$. Fig 1 (Al–Si diagram), Fig 2 (cold work vs. properties, iron and copper) and
Fig 3 (isothermal diagram, 0.8% C steel) are printed in the paper; the values used below were read off them.
Question 5: Copper Wire Drawing — Penultimate Die Diameter for a Strength + Ductility Spec; Dislocations in Cold Rolling (5 of 5)
Given. Finished wire $d_f=0.7$ mm; UTS $>325$ MPa; ductility
$\ge10\%$ EL; starting stock 10 mm rod, reduced by alternating cold draws and anneals;
Fig 2 gives copper’s ultimate strength and elongation against %cold work.
Find. (a) The die diameter of the penultimate draw, i.e. the size the wire is drawn to
and then annealed at, just before the final draw to 0.7 mm. (b) Dislocations and their role in cold
rolling brass.
Approach
An anneal removes all previous cold work but does not change the diameter. So the finished properties
depend only on the cold work of the final draw, from the penultimate (annealed) diameter down to
0.7 mm. Going straight from 10 mm to 0.7 mm would be
$1-(0.7/10)^2=99.5\%$ CW, far off the chart. Steps: read the %CW window that meets both floors on
Fig 2’s copper curves, choose a %CW inside it, then back out the penultimate diameter from
$\%CW=\left[1-(d_f/d_p)^2\right]\times100$ (page-1 formula with $A\propto d^2$).
Strength floor → minimum %CW. On the printed copper ultimate-strength curve
(digitised: $\approx211$ MPa at 0%, $285$ at 20%, $299$ at 25%, $324$ at 35%, $334$ MPa at
40% CW), the 325 MPa line is crossed at
$$\%CW_{\min}\approx35.5\%.$$
Ductility floor → maximum %CW. On the copper elongation curve
($\approx40\%$ at 0%, $22\%$ at 20%, $14.9\%$ at 30%, $11.8\%$ at 35% CW), 10% EL is reached at
$$\%CW_{\max}\approx38\%.$$
The window $35.5\%\le\%CW\le38\%$ exists but is narrow.
Choose the design cold work. The window is only about 3 points wide, so aim inside
it rather than at an edge, so chart-reading and process scatter cannot push the wire out of spec:
$$\boxed{\%CW_{\text{final draw}}=36\%}$$
Check against the curves: UTS $\approx326$ MPa $>325$ and EL $\approx11\%\ge10\%$.
Penultimate die diameter.
$$\%CW=\left(1-\frac{d_f^2}{d_p^2}\right)\times100\ \Rightarrow\ d_p=\frac{d_f}{\sqrt{1-0.36}}=\frac{0.7}{0.800}$$
$$\boxed{d_p\approx0.875\ \text{mm}\ \ (\approx0.88\ \text{mm})}$$
The full window corresponds to $0.872\le d_p\le0.890$ mm. The wire is drawn to this size, annealed,
and then given the final 36% cold draw to 0.7 mm. The earlier draw/anneal cycles from 10 mm do
not affect the finished properties.
(b) What is a dislocation? A dislocation is a line-type crystal defect along which the
regular atomic stacking is disrupted. In its two limiting forms: an edge dislocation is
the edge of an extra half-plane of atoms inserted into the lattice; a screw dislocation is
a helical distortion produced by a shear offset of one part of the crystal relative to another. The
magnitude and direction of the lattice distortion a dislocation carries is captured by its
Burgers vector $\mathbf b$. Dislocations move (glide) along specific close-packed
crystallographic planes and directions (slip systems) under an applied shear stress; this glide
motion is the physical mechanism of plastic (permanent) deformation in crystalline metals.
(b) Role of dislocations in cold-rolling brass. As the brass sheet ($\alpha$-brass,
FCC, 12 $\{111\}\langle110\rangle$ slip systems) is rolled, plastic strain is accommodated entirely by
dislocation glide on these slip systems. Every increment of plastic strain requires new dislocations to be
generated (chiefly by Frank–Read sources operating within grains) and existing dislocations to move
further, so the total dislocation density rises steeply with %CW — from
$\approx10^6$ mm$^{-2}$ in the annealed sheet to $\approx10^9$–$10^{10}$ mm$^{-2}$ after
heavy rolling. As density rises, dislocations increasingly intersect, tangle with one another, and pile up
at grain boundaries and other dislocations on intersecting slip systems; each such obstacle impedes
further dislocation motion, so a progressively larger applied stress is needed to keep deforming the
material. This is exactly the mechanism of strain (work) hardening: the same
dislocation-multiplication process that carries the plastic strain is also what raises the flow stress
(and hence $\sigma_{UTS}$) and lowers the remaining ductility as %CW increases — precisely the
TS-up/ductility-down trend captured in the Fig. 2 curves used in part (a).
[Figure not reproduced: Fig. Q5(a) — copper (solid) and iron (dashed) ultimate strength vs. %cold work, redrawn from the printed Fig 2. The copper curve reaches the 325 MPa floor at $\approx35.5\%$ CW. See the official exam paper.]
[Figure not reproduced: Fig. Q5(a) — copper (solid) and iron (dashed) elongation vs. %cold work, redrawn from the printed Fig 2. The copper curve falls to the 10% EL floor at $\approx38\%$ CW, so only the band $\approx35.5$–$38\%$ CW meets both requirements. See the official exam paper.]
Quantity
Result
Feasible %CW window, final draw
≈ 35.5% – 38%
Design %CW, final draw
36% (UTS ≈ 326 MPa, EL ≈ 11%)
Penultimate die diameter
≈ 0.875 mm (window 0.872–0.890 mm)
(b) Deformation mechanism
Dislocation glide on {111}〈110〉 slip systems; density ↑ ⇒ work hardening