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23-Chem-A2 Unit Operations and Separation Processes · May 2015

Question 2 of 6: Settling Velocity to Minimum-Fluidization Velocity Ratio

Nivaar worked solution (AI-drafted; not reviewed by a licensed engineer)

Notes on this paper

Paper format. National Exams — 04-CHEM-A2 Mechanical and Thermal Operations, May 2015. 3 hours, open book. Six problems (Section A Mechanical Operations: A1–A3; Section B Thermal Operations: B1–B3), each 25 marks; candidates attempt two from each section. All six are worked below for completeness.

Reference texts. McCabe, Smith & Harriott, Unit Operations of Chemical Engineering (7th ed.); Coulson & Richardson, Chemical Engineering Vol. 1 (fluid flow, heat transfer) and Vol. 2 (particle technology, evaporation); Incropera & DeWitt, Fundamentals of Heat and Mass Transfer (8th ed.); Perry's Chemical Engineers' Handbook (9th ed.).

Note on the charts and tables. Page 3 (Fanning friction-factor chart), page 5 (LMTD correction-factor plot) and page 6 (Table B.2, saturated water by pressure) were read from the printed figure. The smooth-pipe friction factor is computed from the Colebrook equation, which the chart plots; the B3 condenser is isothermal on the steam side, so the correction factor is exactly $F=1$; and the B2 saturation temperatures are read from the supplied Table B.2.


Question A2: Settling Velocity to Minimum-Fluidization Velocity Ratio (25 marks)

Question text not reproduced: the examination questions are © Engineers and Geoscientists BC. Open the official past paper (linked at the top of this page) to read the question, then follow the worked solution below.

Given. Uniform spheres fluidized by a liquid; the ratio requested is the free terminal (settling) velocity $u_t$ over the minimum-fluidization superficial velocity $u_{mf}$.

QuantityValue
Void fraction at $u_{mf}$, $\varepsilon_{mf}$0.48
Particle diameter $d_p$3 mm = 0.003 m
Particle density $\rho_p$4200 kg/m³
Liquid viscosity $\mu$$1\times10^{-3}$ N·s/m²
Liquid density $\rho$1100 kg/m³

Find. $u_t/u_{mf}$. (The bed height $l$ cancels because both velocities are superficial.)

at u_mf (bed just lifts) liquid up, u_mf=0.066 m/s u_t=0.501 m/s free settling (dilute)
Figure A2 — Minimum fluidization (bed of voidage 0.48 on the point of suspension) versus free terminal settling of a single sphere; the ratio of the two velocities characterises the operable fluidization window.

Approach. Get $u_{mf}$ from the full Ergun-equation force balance (bed weight = pressure drop) written as a quadratic in $\mathrm{Re}_{mf}$, and $u_t$ from Newton's law for the coarse, high-Reynolds settling regime; both are superficial velocities so $l$ drops out.

  1. Archimedes number. This dimensionless group sets both correlations: $$\mathrm{Ar}=\frac{d_p^3\rho(\rho_p-\rho)g}{\mu^2}=\frac{(0.003)^3(1100)(3100)(9.81)}{(10^{-3})^2}=9.03\times10^{5}.$$
  2. Minimum-fluidization velocity — full Ergun quadratic. At incipient fluidization the pressure drop equals the buoyed bed weight; substituting the Ergun equation gives $$\frac{1.75}{\varepsilon_{mf}^3}\mathrm{Re}_{mf}^2+\frac{150(1-\varepsilon_{mf})}{\varepsilon_{mf}^3}\mathrm{Re}_{mf}-\mathrm{Ar}=0.$$ With $\varepsilon_{mf}=0.48$: $15.82\,\mathrm{Re}_{mf}^2+705.3\,\mathrm{Re}_{mf}-9.03\times10^5=0$, so $\mathrm{Re}_{mf}=217.7$ and $$u_{mf}=\frac{\mathrm{Re}_{mf}\,\mu}{\rho\,d_p}=\frac{217.7(10^{-3})}{1100(0.003)}=0.066\ \mathrm{m/s}.$$ $u_{mf}=0.066\ \mathrm{m/s}$ Because $\mathrm{Re}_{mf}\approx218$ (well outside the laminar range), the inertial Ergun term is essential — a laminar-only estimate would be invalid.
  3. Terminal settling velocity — Newton's law. For a large sphere in the Newton (constant-$C_D\!\approx\!0.44$) regime, $$u_t=1.74\sqrt{\frac{g\,d_p(\rho_p-\rho)}{\rho}}=1.74\sqrt{\frac{9.81(0.003)(3100)}{1100}}=0.501\ \mathrm{m/s}.$$ $u_t=0.501\ \mathrm{m/s}$ Check: $\mathrm{Re}_t=\rho u_t d_p/\mu = 1650$, which lies in Newton's-law range ($10^3<\mathrm{Re}<2\times10^5$), so the assumption is self-consistent.
  4. Form the ratio. $$\frac{u_t}{u_{mf}}=\frac{0.501}{0.066}=7.6.$$ $u_t/u_{mf} \approx 7.6$ The bed height $l$ appears in neither velocity, so it cancels identically. Drag-law sensitivity: $C_D=0.44$ is slightly high at $\mathrm{Re}_t\approx1650$; the standard sphere drag curve (Coulson & Richardson Galileo-number correlation) gives $u_t\approx0.53\ \mathrm{m/s}$ and a ratio of about 8.1, so expect $u_t/u_{mf}\approx7.6$–8.1.
QuantityResult
Archimedes number$9.03\times10^5$
$\mathrm{Re}_{mf}$ (full Ergun)217.7
Minimum fluidization velocity $u_{mf}$0.066 m/s
Terminal velocity $u_t$ (Newton)0.501 m/s ($\mathrm{Re}_t\approx1650$)
Ratio $u_t/u_{mf}$7.6
Check (assumptions): spheres are uniform and monosized; $\varepsilon_{mf}=0.48$ is taken as the packed-bed voidage at incipient fluidization; particle sphericity $\phi_s=1$; the liquid is Newtonian; and the terminal Reynolds number confirms the Newton-law (rather than Stokes or intermediate) settling regime.