23-Chem-A2 Unit Operations and Separation Processes · May 2015
Question 2 of 6: Settling Velocity to Minimum-Fluidization Velocity Ratio
Nivaar worked solution (AI-drafted; not reviewed by a licensed engineer)
Notes on this paper
Paper format. National Exams — 04-CHEM-A2 Mechanical and Thermal Operations, May 2015. 3 hours, open book. Six problems (Section A Mechanical Operations: A1–A3; Section B Thermal Operations: B1–B3), each 25 marks; candidates attempt two from each section. All six are worked below for completeness.
Reference texts. McCabe, Smith & Harriott, Unit Operations of Chemical Engineering (7th ed.); Coulson & Richardson, Chemical Engineering Vol. 1 (fluid flow, heat transfer) and Vol. 2 (particle technology, evaporation); Incropera & DeWitt, Fundamentals of Heat and Mass Transfer (8th ed.); Perry's Chemical Engineers' Handbook (9th ed.).
Note on the charts and tables. Page 3 (Fanning friction-factor chart), page 5 (LMTD correction-factor plot) and page 6 (Table B.2, saturated water by pressure) were read from the printed figure. The smooth-pipe friction factor is computed from the Colebrook equation, which the chart plots; the B3 condenser is isothermal on the steam side, so the correction factor is exactly $F=1$; and the B2 saturation temperatures are read from the supplied Table B.2.
Question A2: Settling Velocity to Minimum-Fluidization Velocity Ratio (25 marks)
Given. Uniform spheres fluidized by a liquid; the ratio requested is the free terminal (settling) velocity $u_t$ over the minimum-fluidization superficial velocity $u_{mf}$.
Quantity
Value
Void fraction at $u_{mf}$, $\varepsilon_{mf}$
0.48
Particle diameter $d_p$
3 mm = 0.003 m
Particle density $\rho_p$
4200 kg/m³
Liquid viscosity $\mu$
$1\times10^{-3}$ N·s/m²
Liquid density $\rho$
1100 kg/m³
Find. $u_t/u_{mf}$. (The bed height $l$ cancels because both velocities are superficial.)
Figure A2 — Minimum fluidization (bed of voidage 0.48 on the point of suspension) versus free terminal settling of a single sphere; the ratio of the two velocities characterises the operable fluidization window.
Approach. Get $u_{mf}$ from the full Ergun-equation force balance (bed weight = pressure drop) written as a quadratic in $\mathrm{Re}_{mf}$, and $u_t$ from Newton's law for the coarse, high-Reynolds settling regime; both are superficial velocities so $l$ drops out.
Archimedes number. This dimensionless group sets both correlations: $$\mathrm{Ar}=\frac{d_p^3\rho(\rho_p-\rho)g}{\mu^2}=\frac{(0.003)^3(1100)(3100)(9.81)}{(10^{-3})^2}=9.03\times10^{5}.$$
Minimum-fluidization velocity — full Ergun quadratic. At incipient fluidization the pressure drop equals the buoyed bed weight; substituting the Ergun equation gives $$\frac{1.75}{\varepsilon_{mf}^3}\mathrm{Re}_{mf}^2+\frac{150(1-\varepsilon_{mf})}{\varepsilon_{mf}^3}\mathrm{Re}_{mf}-\mathrm{Ar}=0.$$ With $\varepsilon_{mf}=0.48$: $15.82\,\mathrm{Re}_{mf}^2+705.3\,\mathrm{Re}_{mf}-9.03\times10^5=0$, so $\mathrm{Re}_{mf}=217.7$ and $$u_{mf}=\frac{\mathrm{Re}_{mf}\,\mu}{\rho\,d_p}=\frac{217.7(10^{-3})}{1100(0.003)}=0.066\ \mathrm{m/s}.$$ $u_{mf}=0.066\ \mathrm{m/s}$ Because $\mathrm{Re}_{mf}\approx218$ (well outside the laminar range), the inertial Ergun term is essential — a laminar-only estimate would be invalid.
Terminal settling velocity — Newton's law. For a large sphere in the Newton (constant-$C_D\!\approx\!0.44$) regime, $$u_t=1.74\sqrt{\frac{g\,d_p(\rho_p-\rho)}{\rho}}=1.74\sqrt{\frac{9.81(0.003)(3100)}{1100}}=0.501\ \mathrm{m/s}.$$ $u_t=0.501\ \mathrm{m/s}$ Check: $\mathrm{Re}_t=\rho u_t d_p/\mu = 1650$, which lies in Newton's-law range ($10^3<\mathrm{Re}<2\times10^5$), so the assumption is self-consistent.
Form the ratio. $$\frac{u_t}{u_{mf}}=\frac{0.501}{0.066}=7.6.$$ $u_t/u_{mf} \approx 7.6$ The bed height $l$ appears in neither velocity, so it cancels identically. Drag-law sensitivity: $C_D=0.44$ is slightly high at $\mathrm{Re}_t\approx1650$; the standard sphere drag curve (Coulson & Richardson Galileo-number correlation) gives $u_t\approx0.53\ \mathrm{m/s}$ and a ratio of about 8.1, so expect $u_t/u_{mf}\approx7.6$–8.1.
Quantity
Result
Archimedes number
$9.03\times10^5$
$\mathrm{Re}_{mf}$ (full Ergun)
217.7
Minimum fluidization velocity $u_{mf}$
0.066 m/s
Terminal velocity $u_t$ (Newton)
0.501 m/s ($\mathrm{Re}_t\approx1650$)
Ratio $u_t/u_{mf}$
7.6
Check (assumptions): spheres are uniform and monosized; $\varepsilon_{mf}=0.48$ is taken as the packed-bed voidage at incipient fluidization; particle sphericity $\phi_s=1$; the liquid is Newtonian; and the terminal Reynolds number confirms the Newton-law (rather than Stokes or intermediate) settling regime.