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23-Chem-A2 Unit Operations and Separation Processes · December 2018

Question 1 of 6: Minimum Area of a Continuous Thickener

Nivaar worked solution (AI-drafted; not reviewed by a licensed engineer)

Notes on this paper

Paper format. 16-CHEM-A2, Unit Operations and Separation Processes — December 2018, 3-hour open-book exam. Six 25-point problems: Part A (Unit Operations) — A1 continuous-thickener sizing, A2 series-pipe friction pressure drop, A3 packed/fluidized-bed pressure drop & power; Part B (Separation Processes) — B1 flash vs. differential distillation, B2 batch-drying time, B3 adsorption isotherm fitting & surface area. The rubric asks for two problems per part; all six are worked in full below.

Reference texts (subject). McCabe, Smith & Harriott, Unit Operations of Chemical Engineering (7th ed.); Coulson & Richardson, Chemical Engineering Vol. 2 (5th ed.); Geankoplis, Transport Processes and Separation Process Principles (4th ed.); Treybal, Mass-Transfer Operations (3rd ed.); Perry's Chemical Engineers' Handbook (§6 fluid & particle mechanics, §12 drying, §16 adsorption, §18 solid–liquid separation).

Question A1: Minimum Area of a Continuous Thickener (25 points)

Question text not reproduced: the examination questions are © Engineers and Geoscientists BC. Open the official past paper (linked at the top of this page) to read the question, then follow the worked solution below.

Given.

Concentration $X$ (kg water/kg solids)Sedimentation rate $u_c$ (mm/s)
5.0 (feed)0.20
4.20.12
3.70.094
3.10.07
2.50.05
Underflow $X_u$1.5
Solids feed rate $W$4788 kg/hr $=1.33$ kg/s

Find. The minimum settling area $A$ (m²) that lets the continuous thickener discharge underflow at $X_u=1.5$ while clarifying the overflow.

Continuous gravity thickener (Coe–Clevenger sizing) clarification zone (overflow) zone-settling / hindered zone compression zone → underflow feed X = 5.0, W = 1.33 kg/s clear overflow thick underflow Xₕ = 1.5
Figure A1 — In each horizontal layer the water released by thickening must rise faster than the settling solids. The required area is the largest of the layer-by-layer demands (Coe–Clevenger); the controlling layer sets the minimum thickener area.

Approach. By the Coe–Clevenger method the area needed to clarify a layer at concentration $X$ is $A=\dfrac{W\,(X-X_u)}{\rho_w\,u_c}$; evaluate it for every test concentration and take the maximum, because the layer with the greatest area demand controls.

  1. Solids mass rate in SI. $W=\dfrac{4788}{3600}=\boxed{1.33\ \text{kg solids/s}}$.
  2. Coe–Clevenger area per layer. The upward volumetric flow of released water in a layer is $W(X-X_u)/\rho_w$; dividing by the settling velocity gives the area, $$A=\frac{W\,(X-X_u)}{\rho_w\,u_c},\qquad \rho_w=1000\ \text{kg/m}^3.$$ Applying it to each test point (with $u_c$ converted mm/s → m/s):
$X$ (kg w/kg s)$X-X_u$$u_c$ (m/s)$A$ (m²)
5.03.5$2.0\times10^{-4}$23.27
4.22.7$1.2\times10^{-4}$29.93
3.72.2$\mathbf{9.4\times10^{-5}}$31.13 ← max
3.11.6$7.0\times10^{-5}$30.40
2.51.0$5.0\times10^{-5}$26.60
  1. Controlling layer and minimum area. The largest demand occurs at $X=3.7$, so $$A_\text{min}=\frac{1.33\,(3.7-1.5)}{1000\,(9.4\times10^{-5})}=\boxed{31.1\ \text{m}^2}.$$ A thickener smaller than this would let solids escape in the overflow at the $X=3.7$ layer; a larger unit is safe but wasteful. The corresponding diameter is $D=\sqrt{4A/\pi}=6.3$ m.
QuantityValue
Solids mass rate $W$1.33 kg/s
Controlling concentration$X = 3.7$ kg water/kg solids
Minimum thickener area31.1 m² ($D \approx 6.3$ m)
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