23-Chem-A2 Unit Operations and Separation Processes · December 2018
Question 1 of 6: Minimum Area of a Continuous Thickener
Nivaar worked solution (AI-drafted; not reviewed by a licensed engineer)
Notes on this paper
Paper format. 16-CHEM-A2, Unit Operations and Separation Processes — December 2018, 3-hour open-book exam. Six 25-point problems: Part A (Unit Operations) — A1 continuous-thickener sizing, A2 series-pipe friction pressure drop, A3 packed/fluidized-bed pressure drop & power; Part B (Separation Processes) — B1 flash vs. differential distillation, B2 batch-drying time, B3 adsorption isotherm fitting & surface area. The rubric asks for two problems per part; all six are worked in full below.
Reference texts (subject). McCabe, Smith & Harriott, Unit Operations of Chemical Engineering (7th ed.); Coulson & Richardson, Chemical Engineering Vol. 2 (5th ed.); Geankoplis, Transport Processes and Separation Process Principles (4th ed.); Treybal, Mass-Transfer Operations (3rd ed.); Perry's Chemical Engineers' Handbook (§6 fluid & particle mechanics, §12 drying, §16 adsorption, §18 solid–liquid separation).
Question A1: Minimum Area of a Continuous Thickener (25 points)
Find. The minimum settling area $A$ (m²) that lets the continuous thickener discharge underflow at $X_u=1.5$ while clarifying the overflow.
Figure A1 — In each horizontal layer the water released by thickening must rise faster than the settling solids. The required area is the largest of the layer-by-layer demands (Coe–Clevenger); the controlling layer sets the minimum thickener area.
Approach. By the Coe–Clevenger method the area needed to clarify a layer at concentration $X$ is $A=\dfrac{W\,(X-X_u)}{\rho_w\,u_c}$; evaluate it for every test concentration and take the maximum, because the layer with the greatest area demand controls.
Solids mass rate in SI. $W=\dfrac{4788}{3600}=\boxed{1.33\ \text{kg solids/s}}$.
Coe–Clevenger area per layer. The upward volumetric flow of released water in a layer is $W(X-X_u)/\rho_w$; dividing by the settling velocity gives the area, $$A=\frac{W\,(X-X_u)}{\rho_w\,u_c},\qquad \rho_w=1000\ \text{kg/m}^3.$$ Applying it to each test point (with $u_c$ converted mm/s → m/s):
$X$ (kg w/kg s)
$X-X_u$
$u_c$ (m/s)
$A$ (m²)
5.0
3.5
$2.0\times10^{-4}$
23.27
4.2
2.7
$1.2\times10^{-4}$
29.93
3.7
2.2
$\mathbf{9.4\times10^{-5}}$
31.13 ← max
3.1
1.6
$7.0\times10^{-5}$
30.40
2.5
1.0
$5.0\times10^{-5}$
26.60
Controlling layer and minimum area. The largest demand occurs at $X=3.7$, so $$A_\text{min}=\frac{1.33\,(3.7-1.5)}{1000\,(9.4\times10^{-5})}=\boxed{31.1\ \text{m}^2}.$$ A thickener smaller than this would let solids escape in the overflow at the $X=3.7$ layer; a larger unit is safe but wasteful. The corresponding diameter is $D=\sqrt{4A/\pi}=6.3$ m.