23-Chem-A5 Chemical Plant Design and Economics · December 2016
Question 2 of 6: Cost of a Distillation-Column Retrofit
Nivaar worked solution (AI-drafted; not reviewed by a licensed engineer)
Notes on this paper
National Exams — December 2016 — 04-Chem-A5 Chemical Plant Design and Economics. Three-hour, closed-book exam; one two-sided aid sheet and an approved calculator permitted. Six equally weighted (20-mark) questions are posed and the candidate answers any five; only the first five are marked. All six are answered below for completeness. Question 1 combines conceptual process-synthesis (reactor and recycle structure for a series-reaction chlorination) with a short economic-potential calculation; Question 2 is a numerical retrofit-costing problem (replacing distillation trays with structured packing); Questions 3–6 are qualitative essays on equipment design procedures, materials of construction, inherently safer design, and equipment-selection factors.
Reference texts: R. Smith, Chemical Process Design and Integration (2nd ed., Wiley) — reaction path, reactor conversion and the recycle structure of the flowsheet, and the economic-potential screen behind Question 1 (the monochlorodecane example is worked there); R.K. Sinnott & G. Towler, Chemical Engineering Design (Coulson & Richardson vol. 6, 6th ed., Butterworth-Heinemann) — the equipment cost correlations and retrofit factors of Question 2, the heat-exchanger and cyclone design procedures (Ch. 12, Ch. 10), materials of construction (Ch. 7), and equipment selection (Ch. 10, 18); T.A. Kletz & P. Amyotte, Process Plants: A Handbook for Inherently Safer Design (2nd ed., CRC) — the inherently-safer-design changes of Question 5; M.S. Peters, K.D. Timmerhaus & R.E. West, Plant Design and Economics for Chemical Engineers (5th ed., McGraw-Hill). Canadian practice per CCOHS and CSA Z767 (Process Safety Management) where jurisdiction matters.
Question 2: Cost of a Distillation-Column Retrofit (20 marks)
Find. The estimated total cost of the revamp project (purchase of new stainless-steel structured packing plus removal of the old trays and installation of the packing).
Approach
Cost the new packing from the capacity–cost correlation (diameter is the size variable; a 30 m column needs six 5 m units), then add the retrofit modification costs, which Table 2.8 expresses as multiples of that new-hardware cost.
Figure 2.1 — The revamp: the 46 m × 1.5 m column body is retained; its 70 sieve trays (0.61 m spacing) are removed and replaced by 30 m of stainless-steel structured packing (six 5 m beds). Only the trays→packing swap is costed.
Number of standard packing units. The correlation is quoted per 5 m of packing height, so a 30 m column requires
$$N=\frac{H}{5}=\frac{30}{5}=6 \text{ units}.$$
Cost of one 5 m unit at the actual diameter. Using $C_e=C_B\,(D/Q_B)^{n}$ with $D=1.5$ m (inside the 0.5–4.0 m validity range):
$$C_{5\,\text{m}}=1.80\times10^{4}\left(\frac{1.5}{0.5}\right)^{1.70}=1.80\times10^{4}\,(3)^{1.70}=1.80\times10^{4}(6.473)=\$116{,}500.$$
Delivered cost of the new hardware (all six units).
$$C_{\text{pack}}=N\,C_{5\,\text{m}}=6\times116{,}500\approx\$699{,}100.$$
Delivered cost of the new SS structured packing: $\boxed{C_{\text{pack}}\approx\$699{,}100}$
Retrofit modification costs (Table 2.8, as multiples of $C_{\text{pack}}$). Removing the old trays to install packing costs
$$C_{\text{rem}}=0.10\,C_{\text{pack}}=0.10(699{,}100)\approx\$69{,}900,$$
and installing the new structured packing costs
$$C_{\text{inst}}=(0.5\!-\!0.8)\,C_{\text{pack}}=\$349{,}600\ \text{to}\ \$559{,}300.$$
Total project cost. Sum the hardware purchase, tray removal and packing installation:
$$C_{\text{tot}}=C_{\text{pack}}\,(1+0.10+f_{\text{inst}})=699{,}100\times(1.60\ \text{to}\ 1.90).$$
$$C_{\text{tot}}\approx\$1.12\ \text{million (low)}\ \text{to}\ \$1.33\ \text{million (high)}.$$
Taking the mid-range installation factor (0.65):
Estimated total project cost: $\boxed{C_{\text{tot}}\approx\$1.22\ \text{million}\ \ (\$1.12\text{–}\$1.33\ \text{million})}$
Cost item
Basis
Amount
New SS structured packing (6 × 5 m)
$6\,C_B(1.5/0.5)^{1.70}$
$\$699{,}100$
Remove old trays, install packing
$0.10\,C_{\text{pack}}$
$\$69{,}900$
Install new structured packing
$(0.5\text{–}0.8)\,C_{\text{pack}}$
$\$349{,}600$ – $\$559{,}300$
Total project cost
$C_{\text{pack}}(1+0.10+f_{\text{inst}})$
$\$1.12$ M – $\$1.33$ M (≈ $\$1.22$ M)
Check: the estimate assumes the column body, reboiler, condenser and feed/liquid-distribution internals are adequate for the new duty, so only the trays→packing exchange is costed; the correlation and retrofit factors are order-of-magnitude (study-grade, roughly ±30 %) figures, hence the answer is reported as a range with a best estimate near $\$1.2$ million. The high diameter exponent (1.70) reflects that structured-packing cost scales roughly with cross-sectional area (and the packing value it contains), not just diameter.