23-Chem-A2 Unit Operations and Separation Processes · May 2016
Question 6 of 6: Additional Magnesia Insulation on a Hot Pipe
Nivaar worked solution (AI-drafted; not reviewed by a licensed engineer)
Notes on this paper
Paper format. National Exams — 04-CHEM-A2 Mechanical and Thermal Operations, May 2016. 3 hours, open book. Six problems (Section A Mechanical Operations: A1–A3; Section B Thermal Operations: B1–B3), each 25 marks; candidates attempt at least two from each section (only the first two per section are marked). All six are worked below for completeness.
Reference texts. Coulson & Richardson, Chemical Engineering Vol. 2 (particle technology, sedimentation, fluidization, filtration, crystallization, evaporation) and Vol. 1 (heat transfer); McCabe, Smith & Harriott, Unit Operations of Chemical Engineering (7th ed.); Geankoplis, Transport Processes and Separation Process Principles (4th ed.); Incropera & DeWitt, Fundamentals of Heat and Mass Transfer (8th ed.); Perry's Chemical Engineers' Handbook (9th ed.).
Note on saturation data. Sections B2 and B3 need water saturation temperatures and latent heats that the exam expects from an open-book steam table. These are taken from standard tables (and, for reproducibility). The B1 latent heat of evaporation is not printed in the exam and is taken as 2370 kJ/kg at the cooling range; this and other engineering choices are flagged in Check callouts.
Question B3: Additional Magnesia Insulation on a Hot Pipe (25 marks)
Find. The magnesia thickness $t=r_3-r_2$, and a check that the magnesia stays below 615 K.
Figure B3 — Two conduction resistances in series (existing insulation then magnesia) discharge to air through a combined convection/radiation coefficient; the added magnesia must drop the outer face to 370 K.
Approach. At steady state the same heat rate per metre passes through both conduction layers and off the outer surface; equating the conduction expression (1100 K to 370 K) with the surface loss ($h$, air) gives one equation for the outer radius $r_3$, hence the thickness — then check the magnesia hot-face temperature.
Heat loss set by the target surface. With the outer face fixed at $T_3=370$ K, the surface loss per metre is $$q=h(2\pi r_3)(T_3-T_{air})=10(2\pi r_3)(370-280).$$ This grows with $r_3$.
Same $q$ through the two conduction layers. From 1100 K to 370 K across the series resistance, $$q=\frac{1100-370}{\dfrac{\ln(r_2/r_1)}{2\pi k_1}+\dfrac{\ln(r_3/r_2)}{2\pi k_2}}.$$ This falls as $r_3$ grows (thicker magnesia).
Solve for the outer radius. Equating the two expressions gives a single transcendental equation in $r_3$; numerically $$r_3=0.0924\ \mathrm{m}\;\Rightarrow\; t=r_3-r_2=0.0924-0.075=\;\boxed{17.4\ \mathrm{mm}}.$$ The corresponding loss is $q=522$ W per metre of pipe.
Check the magnesia service temperature. The temperature at the magnesia hot face (inner radius $r_2$) is $$T_{r_2}=1100-q\,\frac{\ln(r_2/r_1)}{2\pi k_1}=1100-522\frac{\ln(3)}{2\pi(0.17)}=563\ \mathrm{K}.$$ Since $563 \mathrm{K}<615 \mathrm{K}$, the magnesia operates safely. Magnesia thickness ≈ 17.4 mm; hot face 563 K < 615 K limit
Quantity
Result
Outer radius $r_3$
92.4 mm
Magnesia thickness $t$
≈ 17.4 mm
Heat loss $q$
522 W/m
Magnesia hot-face T
563 K (< 615 K ✓)
Check (interpretation): the 50 mm pipe "outer diameter" is taken as $r_1=25$ mm with the pipe metal at 1100 K, and the first 50 mm insulation therefore extends to $r_2=75$ mm; the single coefficient $h=10$ W/m²·K lumps convection and radiation at the outer face as the exam states.