23-Chem-A2 Unit Operations and Separation Processes · December 2017
Question 3 of 6: Critical Particle Size in a Settling Lagoon
Nivaar worked solution (AI-drafted; not reviewed by a licensed engineer)
Notes on this paper
Paper format. National Exams — 16-CHEM-A2 Unit Operations and Separation Processes, December 2017. 3 hours, open book (one text). Six problems — Part A Unit Operations (A1–A3) and Part B Separation Processes (B1–B3), each worth 25 marks; the rubric asks for at least two problems from each part (only the first two per part are marked). All six are worked below for completeness as a study resource.
Reference texts. McCabe, Smith & Harriott, Unit Operations of Chemical Engineering (7th ed.); Geankoplis, Transport Processes and Separation Process Principles (4th ed.); Coulson & Richardson, Chemical Engineering Vol. 2 (particle technology, absorption, drying, crystallization); Treybal, Mass-Transfer Operations (3rd ed.); Perry's Chemical Engineers' Handbook (9th ed.).
Notes on chart / model reads. A1's minor-loss balance uses the Blasius smooth-pipe friction factor $f=0.079\,Re^{-0.25}$ (Fanning) — valid to $Re\approx10^5$, and all three test points fall in $3.8$–$8.9\times10^4$; the 1.5 m is taken as the head lost across the pipe-and-valve test section, because also charging an exit velocity head would make the measured open-valve flow physically impossible (see A1). B1(b) reads the Sherwood/Eckert flooding line supplied with the paper at abscissa $0.061$, giving flooding ordinate $\approx0.17$ (graphical, $0.16$–$0.18$), with the tabulated packing factor $F=160\ \text{ft}^{-1}$ converted to $525\ \text{m}^{-1}$ for the SI form of the ordinate. B3(a) sizes the vessel from its starting liquor volume, allowing for the water evaporated during the batch. Engineering choices are flagged in Check callouts.
Part A — Unit Operations
Question A3: Critical Particle Size in a Settling Lagoon (25 marks)
Find. The smallest ore-particle diameter the lagoon can capture (and a check that Stokes' law applies).
Figure A3 — A particle is captured if it settles from surface to floor within its residence time; the cut is set by the overflow rate $Q/A_\text{plan}$, independent of depth.
Approach. A continuous basin captures a particle whenever its terminal settling velocity exceeds the overflow rate $Q/A_\text{plan}$; set the two equal, invert Stokes' law for the diameter, and confirm $Re_p<0.4$.
Overflow (surface-loading) rate. The basin is an ideal clarifier, so the cut velocity is the flow divided by the plan area (depth cancels): $$v_t^{\,\text{crit}}=\frac{Q}{A_\text{surface}}=\frac{0.10\ \text{m}^3/\text{s}}{(10)(50)\ \text{m}^2}=\boxed{2.0\times10^{-4}\ \text{m/s}}.$$ Any particle settling faster than this reaches the floor before the outlet.
Invert Stokes' law for the critical diameter. The smallest retained particle settles at exactly $v_t^{\,\text{crit}}$. From $v_t=\dfrac{g\,d^2(\rho_p-\rho_f)}{18\mu}$, $$d=\sqrt{\frac{18\mu\,v_t}{g(\rho_p-\rho_f)}}=\sqrt{\frac{18(1\times10^{-3})(2.0\times10^{-4})}{9.81(2800-1000)}}=\boxed{1.43\times10^{-5}\ \text{m}=14.3\ \mu\text{m}}.$$
Check the Stokes-law validity. The particle Reynolds number at this size is $$Re_p=\frac{\rho_f\,v_t\,d}{\mu}=\frac{1000(2.0\times10^{-4})(1.43\times10^{-5})}{1\times10^{-3}}=2.9\times10^{-3}\ \ll0.4.\ \checkmark$$ Deeply viscous — Stokes' law is fully valid.
Model bound. The largest size for which Stokes still holds ($Re_p=0.4$) is $d_\text{max}=\left[\dfrac{0.4(18)\mu^2}{\rho_f g(\rho_p-\rho_f)}\right]^{1/3}\approx74\ \mu\text{m}$. The 14.3 µm cut lies well inside the valid range, so the answer is self-consistent: the lagoon retains ore $\gtrsim14.3\ \mu\text{m}$ and finer particles overflow.