23-Chem-A2 Unit Operations and Separation Processes · May 2017
Question 1 of 6: Sizing a Flow Nozzle for an Ethanol Line
Nivaar worked solution (AI-drafted; not reviewed by a licensed engineer)
Notes on this paper
Paper format. National Exams — 16-CHEM-A2 Unit Operations and Separation Processes, May 2017. 3 hours, open book (one text). Six problems — Part A Unit Operations (A1–A3) and Part B Separation Processes (B1–B3), each worth 25 marks; the rubric asks for at least two problems from each part (only the first two per part are marked). All six are worked below for completeness as a study resource.
Reference texts. McCabe, Smith & Harriott, Unit Operations of Chemical Engineering (7th ed.); Geankoplis, Transport Processes and Separation Process Principles (4th ed.); Coulson & Richardson, Chemical Engineering Vol. 2 (particle technology, filtration, crystallization, drying, absorption); Perry's Chemical Engineers' Handbook (9th ed.); Badger & Banchero, Introduction to Chemical Engineering.
Notes on chart / table reads. A1 uses the ISO nozzle discharge-coefficient chart ($C_n$ vs $Re$, $\beta$); B1's isotherm concentrations are printed as “g/cm³” but are read as g/L (= kg/m³) so the feed concentration (0.25 kg/m³) sits on the same scale as the data — a units slip in the source; B3's equilibrium $Y$ column carries an implied ×10−4 multiplier (the printed integers 0–202 cannot be literal mol/mol, and the inlet gas $Y_1=0.0177$ coincides exactly with the $X=10$ entry of 177, which fixes the scale). Engineering choices are flagged in Check callouts.
Part A — Unit Operations
Question A1: Sizing a Flow Nozzle for an Ethanol Line (25 marks)
Find. The throat (nozzle) diameter $d$ that produces exactly 4 kPa at the design flow.
Figure A1 — ISO flow nozzle. The throat diameter $d$ (ratio $\beta=d/D$) sets both the metering area and the discharge coefficient $C_n(Re,\beta)$ read from the chart.
Approach. The pipe-based Reynolds number is fixed by the given flow, so the discharge coefficient depends only on the unknown diameter ratio $\beta=d/D$; iterate the nozzle-meter equation with $C_n$ read from the chart until $d$ is self-consistent.
Pipe velocity and Reynolds number. The approach velocity is $$v=\frac{Q}{\tfrac{\pi}{4}D^2}=\frac{3\times10^{-3}}{\tfrac{\pi}{4}(0.060)^2}=1.061\ \mathrm{m/s},$$ so $$Re=\frac{\rho v D}{\mu}=\frac{(789)(1.061)(0.060)}{1.19\times10^{-3}}=\boxed{4.22\times10^{4}}.$$ This is set by the pipe and the flow — it does not change as we vary the throat.
Nozzle-meter equation. For a flow nozzle the metered flow is $$Q=C_n\,\frac{\pi}{4}d^{2}\,\sqrt{\frac{2\,\Delta p}{\rho\,(1-\beta^{4})}},\qquad \beta=\frac{d}{D}.$$ The velocity-of-approach factor $1/\sqrt{1-\beta^4}$ corrects for the finite upstream velocity. Rearranging for the throat area, $$d^{2}=\frac{Q\,\sqrt{1-\beta^{4}}}{C_n\,\tfrac{\pi}{4}\sqrt{2\Delta p/\rho}}.$$
Read the discharge coefficient. At $Re=4.2\times10^{4}$ the chart curves are still rising. Taking a first guess $\beta\approx0.57$, the interpolated $\beta\!=\!0.6$ curve reads $C_n\approx0.98$. With $\sqrt{2\Delta p/\rho}=\sqrt{2(4000)/789}=3.184\ \mathrm{m/s}$.
Iterate to a consistent diameter. Starting from $\beta=0.57$, $\sqrt{1-\beta^4}=0.946$: $$d^{2}=\frac{(3\times10^{-3})(0.946)}{(0.98)(0.7854)(3.184)}=1.16\times10^{-3}\ \mathrm{m^2}\Rightarrow d=0.0340\ \mathrm{m}.$$ Then $\beta=0.0340/0.060=0.567$, which reproduces the assumed $C_n$ — the loop has converged in one pass. $$\boxed{d\approx34\ \mathrm{mm}\quad(\beta=0.57)}$$