Nivaar worked solution (AI-drafted; not reviewed by a licensed engineer)
Notes on this paper
National Exam 04-BS-11, Properties of Materials — December 2015. 3 hours,
closed-book examination (approved Casio or Sharp calculator only). Candidates attempt five,
and only five, questions for a full paper: two from Section A, two from Section B, and the
fifth from either section. All eight questions are solved below for completeness.
Given. (a) TTT diagram for 1035 steel (Fig 2), with hardness values
correlated to hold temperature for fully transformed structures ($1100^\circ$F→240 HB,
$1000^\circ$F→300 HB, $M_s=600^\circ$F, $M_f=490^\circ$F). (b) $\sigma_y=600$ MPa,
$K_{IC}=120$ MPa$\cdot$m$^{1/2}$, applied stress $\le0.70\sigma_y$.
Find. (a)(i) Two candidate as-cast microstructures giving 400 HB. (a)(ii)
A time-temperature path achieving ≤250 HB. (b) Minimum (critical) crack size and
applicable NDT methods.
(a)(i) As-cast 400 HB structures. Reading Fig 2's hardness scale,
400 HB sits at the $M_s$ line ($600^\circ$F), i.e. in the hardest region the diagram
documents. An as-cast part that air-cools moderately quickly (especially a thin section) can
easily miss the pearlite "nose" and transform at low temperature without a controlled isothermal
hold, so two plausible as-cast microstructures giving this hardness are
(untempered) martensite (if the local cooling rate carried the section past the
nose and down through $M_s$–$M_f$) and lower bainite (if the cooling rate
was fast enough to avoid the pearlite nose but not fast enough to reach $M_s$, so the material
isothermally-in-effect transforms in the low-temperature bainite range on the way down) —
both are hard, brittle, difficult-to-machine products consistent with an uncontrolled as-cast
cooling path.
(a)(ii) Choosing the isothermal hold temperature. Interpolating Fig 2's
hardness correlation between $1100^\circ$F (240 HB) and $1000^\circ$F (300 HB), a
target of 250 HB max falls just below $1100^\circ$F. Holding at
$$\boxed{T_{hold}=1100^\circ\text{F}\ (\approx240\ \text{HB, well inside the }\le250\text{ HB spec})}$$
is the practical choice: it is also the temperature of the curve's nose (the fastest-transforming
temperature), so it minimizes the required furnace/hold time and produces the softest, coarsest
pearlite the diagram documents.
Reading the isothermal hold time. At $1100^\circ$F transformation
starts at the nose of the start curve, $t\approx100$ s, and the finish curve is
reached at its own nose, so transformation is complete by
$$t_{hold}\approx600\ \text{s}\quad(\approx10\ \text{min})$$
(a chart reading, disclosed as approximate to the precision the reproduced curve supports).
Fig. Q5a(ii) — isothermal anneal path: rapid quench from the
austenitizing temperature to 1100°F, hold for ≈600 s (to the finish curve, giving
100% coarse pearlite at ≈240 HB), then air cool to room temperature (no further
transformation occurs on final cooling since the structure is already fully transformed).
(b) Critical crack size. With the page-1 fracture-toughness formula
$K_{IC}=f\sigma\sqrt{\pi a}$ and assuming the standard geometry factor $f=1$ (no other geometry is
specified), the applied stress is
$$\sigma=0.70\times600=420\ \text{MPa},$$
and solving for the crack size $a$ at the point of failure ($K=K_{IC}$):
$$a=\frac{1}{\pi}\left(\frac{K_{IC}}{f\sigma}\right)^2
=\frac{1}{\pi}\left(\frac{120}{420}\right)^2$$
$$\boxed{a\approx26\ \text{mm}}$$
(the half-length of an internal flaw, or the full depth of an edge/surface flaw, under this
$f=1$ convention — i.e. a total internal crack length of ≈52 mm).
Detection methods for a ≈25–50 mm crack. A flaw of this size is
macroscopic and well within the resolving power of standard NDT: radiography
(X-ray or $\gamma$-ray, showing internal flaws as a density/absorption contrast on film or a
digital detector), ultrasonic testing (a pulse-echo probe detects the crack as a
reflected/back-scattered signal, and can also size and depth-locate it), and, if the crack
reaches the surface, the faster and cheaper magnetic particle inspection (for
this ferromagnetic low-alloy steel — iron filings/ink concentrate at the leakage flux over a
surface-breaking crack) or dye penetrant inspection. Any of these would readily
detect a crack well below the ≈25–50 mm critical size, giving a real inspection
margin before the tank reaches the failure condition.